Radiometric calibration of radiation detectors at PTB using synchrotron radiation is based on
the utilisation of cryogenic radiometers as primary detector standards. Different beamlines provides continuously tunable
monochromomatised synchrotron radiation for detector based radiometry in the wavelengths regions of the vacuum-ultraviolet
(VUV), extreme ultraviolet (EUV), and x-rays. For the different regions, different types of photodiodes has proven to be
suited best for defining a scale of spectral responsivity, e. g. Schottky-type PtSi-nSi diodes in the VUV range, or nSi-pSi
diodes in the EUV and x-ray range. The selection of the photodiodes particularly depends on their characteristics concerning
stability, homogeneity and linearity. Calibration of the detectors is realized by comparison of the detector signal with the
incident radiant power of the dispersed synchrotron radiation determined by the cryogenic radiometer. The largest uncertainty
contributions to this process come from the detector itself and from the stray- and false light effects in the monochromatized
synchrotron radiation beam. PTB maintains and disseminates a scale of spectral responsivity with synchrotron radiation between 3 eV and
60 keV (see figure). Based on this, PTB offers a certified calibration service to customers, for the radiometric calibration
of suitable photodetectors, e. g. semiconductor photodiodes, photocathodes, or CCD devices.
Scale of spectral responsivity in the VUV and x-ray range for different type of
semiconductor photodiodes (Click to enlarge)
References
A. Gottwald, U. Kroth, M. Krumrey, M. Richter, F. Scholze, G. Ulm
The PTB High-Accuracy Spectral Responsivity Scale in the VUV and X-Ray Range
Metrologia 43, S125-S129 (2006)
M. Gerlach, M. Krumrey, L. Cibik, P. Müller, H. Rabus, G. Ulm
Cryogenic Radiometry in the Hard X-Ray Range
Metrologia 45, 577-585 (2008)