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FachabteilungenAbt. 3 Chemische Physik und Explosionsschutz 3.1 Metrologie in der Chemie > Veröffentlichungen
Metrologie in der Chemie
Fachbereich 3.1

Veröffentlichungen / Publications (3.1)

Eine vollständige Übersicht der Publikationen finden Sie in der Datenbank PTB-Publica.

2012
Pramann, A.; Rienitz, O.; Schiel, D.: Silicon isotope ratios affected by solium-induced broadband interference in high resolution MC-ICP-MS. Analytical Chemistry (2012)
Pramann, A.; Rienitz, O.; Schiel, D.; Güttler, B.: Avogadro’s number revisited by high resolution inductively-coupled-plasma mass spectrometry. Konferenzbeitrag: Bunsentagung 2012, Leipzig, 17.-19.05.2012, Bunsen-Magazin 14, p. 199 (2012)
Frank, C.; Rienitz, O.; Jährling, R.; Schiel, D., Zakel, S.: Reference measurement procedures for the iron saturation in human transferrin based on IDMS and Raman scattering. Metallomics, 4, S. 1239-1244 (2012)
Sommer, K.-D.; Spitzer, P.; Ebert, V.: New challenges in environmental metrology.  Konferenzbeitrag: XX IMEKO World Congress, Metrology for Green Growth, Busan, Republic of Korea, 10.-14.09.2012
Stosch, R.; Zakel, S. Molecular Fingerprints-Isotope dilution in quantitative Raman Spectrometry. Labor & More (Special Edition) 2.12, 2012
Swart, C.; Fisicaro, P.; Goenaga-Infante, H.; Zakel, S.: Metalloproteins – a new challenge for metrology. Metallomics, Advance Article, 2012
Rienitz, O.; Hauswaldt, A.-L.; Jährling, R.: Solution to standard addition challenge. Analytical and Bioanalytical Chemistry, Springer (2012) 404:2117-2118
Brodehl, A.; Dieding, M.; Cakar, H.; Klauke, B:; Walhorn, V:; Gummert, Jan; Anselmetti, D:; Milting, Hendrik: Functional characterization of desmin mutant p.P419S. European Journal of Human Genetics (2012)
Arsene, C.G.;  Schulze, D.;  Kratzsch, J.; Henrion, A.: High Sensitivity Mass Spectrometric Quantification of Serum Growth Hormone by Amphiphilic Peptide Conjugation. J Mass Spectrom. 47, 1554-1560 (2012)
Seitz, S.; Spitzer, P.; Durbiano, F.; Jensen, H.: Electrolytic conductivity as a quality indicator for bioethanol. Konferenzbeitrag: XX IMEKO World Congress, Metrology for Green Growth, Busan, Republic of Korea, 10.-14.09.2012
Stoica , D.;  Fisicaro, P.; Spitzer, P.; Adel, B.;  Gonzaga, F.B.; Fraga, I.C.; Borges, P.P.; Maksimov, I.; Asakai, T.; Hioki, A.: Determination of pH values for reference patassium hydrogen phthalate buffer in water-ethanol mixture (mass fraction 50 %). Konferenzbeitrag: XX IMEKO World Congress, Metrology for Green Growth, Busan, Republic of Korea, 10.-14.09.2012
Rienitz, O.; Schiel, D.; Görlitz, V.; Jährling, R.; Vogl, J.; Lara-Manzano, J.V.; Zon, A.; Fung, W.-h.; Buzoianu, M.; Caciano de Sena, R.; Augusto dos Reis, L.; Valiente, L.; Yim, Y.-H.; Hill, S.; Chamion, R.; Fisicaro, P.; Bing, W.; Turk, G.C.; Winchester, M.R.; Saxby, D.; Merrick, J.; Hioki, A.; Miura, T.; Suzuki, T.; Linsky, M.; Barzev, A.; Máriássy, M.; Cankur, O.; Ari, B.; Tunc, M.; Konopelko, L.A.; Kustikov, Y.A.; Bezruchko, M.: Final report on CCQM-K87: Mono-elemental calibration solutions. Metrologia 49 (2012)
Meija, J.; Mester, Z.; Pramann, A.; Rabb, S.; Rienitz, O.; Schiel, D.; Sturgeon, R.; Turk, G.; Vocke Jr., R.; Yang, L.: On the Molar Mass of Silicon for a New Avogadro Constant. Conference on Precision Electromagnetic Measurements, 01.-06.07.2012, Washington, USA, Digest IEEE, pp. 476–477
Friedemann, Miriam; Woszczyna, Miroslaw; Müller, André; Wundrack, Stefan; Dziomba, Thorsten; Weimann, Thomas; Ahlers; Franz: Versatile sputtering technology for Al2O2 gate insulators on graphene. Science and Technology of Advanced Materials, 2012, 13
Stosch, R.; Zakel, S.: Isotopenverdünnung in der quantitativen Ramanspektrometrie-Molekulare Fingerabdrücke, labor&more 2012 (4) 40-44
Rienitz, O.; Hauswaldt, A.-L.; Jährling, R.: Standard addition challenge. Analytical and Bioanalytical Chemistry (2012) 403:2461-2462
Becker, P.; Borys, M.; Gläser, M.; Güttler, B.; Schiel, D.: Masse und Stoffmenge – Die Si-Basiseinheiten Kilogramm und Mol. PTB-Mitteilungen: 122 (2012), Heft 1, S. 37-57
Magnusson, B.; Ossowicki, H.; Rienitz, O.; Theodorsson, E.: Routine internal- and external-quality control data in clinical laboratories for estimating measurement and diagnostic uncertainty using GUM principles. Scandinavian Journal of Clinical & Laboratory Investigation (2012) 72: 212-220
Hauswaldt, A.-L.; Rienitz, O.; Jährling, R.; Fischer, N.; Schiel, D.; Labarraque, G.; Magnusson, B.: Uncertainty of standard addition experiments: a novel approach to include the uncertainty associated with the standard in the model equation. Accreditation and Quality Assurance, 2012, 17:129-138
2011
Spitzer, P.; Adel, B.; Meyer, J.; Matzke, J.; Gonzaga, F. B.; Borges, P. P.; Dias, J. C.; Hongyu, X.; Bing, W.; Jakobsen, P . T.; Champion, R.; Ohata, M.; Maksimov, I.; Hioki, A.; Vyskocil, L.; Mariassy, M.; Pratt, K.: Final Report on CCQM-K19.1: pH of borate buffer. Metrologia 48 (2011)
Hauswaldt, A.-L.; Rienitz, O.; Jährling, R.: Standardaddition mit gravimetrischer Präparation und innerem Standard -  Berücksichtigung der Messunsicherheit des addierten Standards. 5. VDI-Fachtagung Messunsicherheit praxisgerecht bestimmen, Erfurt, 08.-09.11.2011, VDI-Berichte 2149, 2011
Rienitz, O.; Pramann, A.; Hauswaldt, A.-L.: Berücksichtigung von Korrelationen bei der Messung von Isotopenverhätlnissen mit simultaner Detektion. 5. VDI-Fachtagung Messunsicherhet praxisgerecht bestimmen, Erfurt, 08.-09.11.2011, VDI-Berichte 2149, 2011
Schiel, D.; Rienitz, O.; Jährling, R.; Güttler, B.; Matschat, R.; Scharf, H.; Birkhahn, J.; Labarraque, G.; Fisicaro, P.; Quetel, C.; Borchers, U.; Schwesig, D.: Metrological concept for comparable measurement results under the Water Framework Directive – Demonstration of its applicability in elemental analysis. Accreditation and Quality Assurance (AQUAL), 2011, 16:489-498
Swart, C.; Rienitz, O.; Schiel, D.: Impact of pump flow fluctuations on post column online ID-ICP-MS. Analytical and Bioanalytical Chemistry 401 (2011), 6, 2025-2031
Zakel, S.; Rienitz, O.; Güttler, B.; Stosch, R.: Double Isotope Dilution Surface-enhanced Raman Scattering as a Reference Procedure for the Quantification of Biomarkers in Human Serum. Analyst, 2011, 136 (19), 3956-3961
Abou-El-Sherbini, K.S.; Schiel, D.; Stosch, R.; Weidler, P.G.: Stabilization of quercetin - functionalized silica gel against hydrolysis by blocking silanol groups with TiO2 or ZrO2 and its application for the removal of Hg(II). Journal of Sol-Gel Science and Technology 57 (2011), 1, 57-67
Swart, C.; Rienitz, O.; Schiel, D.: Alternative approach to post column online isotope dilution ICP-MS. Talanta (The international Journal of Pure and Applied Analytical Chemistry) Vol. 83, No. 5 (2011), S. 1544-1551
Stosch, R.; Yaghobian, F.; Weimann, Th.; Brown, R.J.C.; Milton, M.J.T.; Güttler, B.: Lithographical gap-size engineered nanoarrays for surface-enhanced Raman probing of biomarkers. Nanotechnology 22 (2011) 105303
Nwaboh, Javis A.; Werhahn, Olav; Schiel, D.: Measurement of CO amount fractions using a pulsed quantum-cascade laser operated in the intra-pulse mode. Applied Physics B: 103 (2011), 4, 947-957
Pramann, A.; Rienitz, O.; Schiel, D.; Güttler, B.: Novel concept for the mass spectrometric determination of absolute isotopic abundances with improved measurement uncertainty: Part 2 – Development of an experimental procedure for the determination of the molar mass of silicon using MC-ICP-MS. International Journal of Mass Spectrometry (Int. J. Mass Spectrom) (2011) 299:78-86
Nwaboh, Javis; Werhahn, Olav; Schiel, Detlef; Desbois, T.; Romanini, D.: Molecular laser spectroscopy as a tool for gas analysis applications. International Journal of Spectroscopy: (2011), S. 12
Zakel, Sabine; Wundrack, Stefan; Niemann, Henning; Rienitz, Olaf; Schiel, Detlef: Infrared spectrometric measurement of impurities in highly enriched Si28. Metrologia 48 (2011) S. 14-19
Massa, E.; Mana, G.; Ferroglio, L.; Kessler, E.G.; Schiel, D.; Zakel, S.: The lattice parameter of the 28Si spheres in the determination of the Avogadro constant, Metrologia 48 (2011) S. 44-49
Andreas, B.; Azuma, Y.; Bartl, G.; Becker, P.; Bettin, H.; Borys, M.; Busch, I.; Gray, M.; Fuchs, P.; Fujii, K.; Fujimoto, H.; Kessler, E.; Krumrey, M.; Kuetgens, U.; Kuramoto, N.; Mana, G.; Manson, P.; Massa, E.; Mizushima, S.; Nicolaus, A.; Picard, P.; Pramann, A.; Rienitz, O.; Schiel, D.; Valkiers, S.; Waseda, A.: Determination of the Avogadro constant by counting the atoms in a 28Si crystal. Physical Review Letters: 106 (2011), 3
Andreas, B., Azuma, Y., Bartl, G., Becker, P., Bettin, H., Borys, M., Busch, I., Fuchs, P., Fujii, K.,  Fujimoto, H., Kessler, E., Krumrey, M., Kuetgens, U., Kuramoto, N., Mana, G., Manson, P., Massa, E., Mizushima, S., Nicolaus, A., Picard, A. ,Pramann, A., Rienitz, A., Schiel, D., Valkiers, S., Waseda, A., and Zakel, S.: Counting the atoms in a 28Si crystal for a new kilogram definition. Metrologia, (2011) 48:1
Pramann, A.; Rienitz, O.; Schiel, D.; Schlote, J.; Güttler, B.; Valkiers, S.: Molar mass of silicon highly enriched in 28Si determined by IDMS. Metrologia (2011) 48:20
Bulska, E.; Drozdov, M. N.; Mana, G.; Pramann, A.; Rienitz, O.; Sennikov, P.; Valkiers, S.: The molar mass of enriched Si: a data analysis. Metrologia (2011) 48: 32
Nottbohm, C. T.; Turchanin, A.; Beyer, A.; Stosch, R.; Gölzhäuser, A.: Mechanically Stacked 1-nm-Thick Carbon Nanosheets: Ultrathin Layered Materials with Tunable Optical, Chemical and Electrical Properties, Small, 7 ( 2011) 874-883
Hauswaldt, A.-L.; Rienitz, O.; Jährling, R.; Fischer, N.; Schiel, D.; Labarraque, G.; Mangusson, B.: Uncertainty of standard addition experiments: a novel approach to include the uncertainty associated with the standard in the model equation. Accreditation and Quality Assurance 2011, 16
Yaghobian, F.; Weimann, Th.; Güttler, B.; Stosch, R.: On-chip approach for traceable quantification of biomarkers based on isotope-dilution surface-enhanced Raman scattering (IDSERS). Lab on a Chip (2011), 11, 2955-2960
Turchanin, A.; Weber, D.; Büenfeld, M.; Kisielowski, C.; Fistul, M.; Efetov, K.; Weimann, T.; Stosch, R.; Mayer, J.; Gölzhäuser, A.: Conversion of Self-Assembled Monolayers into Nanocrystalline Graphene: Structure and Electric Transport. ACS Nano 5 (2011) 3896-3904
Stosch, R.; Zakel, S.; Yaghobian, F.; Wundrack, S.; Weimann, T.; Güttler, B.: Oberflächenverstärkte Ramanstreuung – Anwendung metallischer Nanostrukturen für die Metrologie in der Chemie, PTB-Mitteilungen 121 (2011), Heft 2, 137-140
Pramann, A.; Rienitz, O.; Schiel, D.; Güttler, B.; Valkiers, Staf: Novel concept for the mass spectrometric determination of absolute isotopic abundances with improved measurement uncertainty: Part 3 – Molar mass of silicon highly enriched in 28Si. International Journal of Mass Spectrometry (2011) 305:58-68
Schiel, D.; Rienitz, O.: Final report on CCQM-K70: Determination of Hg in natural water at a concentration level required by the European environmental quality standard (EQS). Metrologia, 48 (2011)
Seitz, St.; Spitzer, P.; Feistel, R.; Weinreben, St.; Wright, D.; De Bièvre, P.: Metrological Traceability of Oceanographic Salinity measurement results. Ocean Science 7 (2011), 45-62
Spitzer, Petra; Fisicaro, Paola; Meinrath, Günther; Stoica, Daniela: pH buffer assessement and Pitzer’s equations. Accreditation and Quality Assurance (AQUAL) (2011) 16:191-198
Spitzer, P.; Pratt, Kenneth W.: The history and development of a rigorous metrological basis for pH measurements. J. Solid State Electrochem (2011) 15:69-76
Marion, G.M.; Millero, F.J.; Camões, M.F.; Spitzer, P.; Feistel, R.;Chenf, C.T.A.: pH of Seawater. Marine Chemistry (2011)
Spitzer, P.; Seitz, S.: Electrolytical Conductivity. [Buchkapitel] Springer Handbook of Metrology and Testing, 2nd. ed. 2011, Chapter 9.3, pp. 498-507, Editors : Czichos, H.; Saito, T.; Smith, L.
Spitzer, P.; Sommer; K.-D.: The metrological challenge in earth observation. IMEKO MI 2011, Dubrovnik Riviera, Cavtat, Croatia, 15.–17.06.2011
2010
Arsene, C.: Wachstumshormon im Serum per IDMS bestimmen. LaborPraxis (Journal für Labor, Analytik und Life Sciences), Ausgabe 12-2010, S. 28
Spitzer, P.; Seitz, S.: Metrological traceability chain for pH measurement results. MAPAN, Journal of Metrology Society of India (2010) Volume 25, Number 3, 191-196
Güttler, B.; Richter, W.: Metrology in Chemistry in Germany. CMW-2009; MAPAN: 25 (2010), 3, 219-225
Rienitz, O.; Pramann, A.; Schiel, D.: Novel concept for the mass spectrometric determination of absolute isotopic abundances with improved measurement uncertainty: Part 1 – theoreticall derivation and feasibility study. International Journal of Mass Spectrometry 289 (2010) 47-53
Mana, G.; Rienitz, O.: The calibration of Si isotope-ratio measurements. International Journal of Mass Spectrometry 291 (2010) 55-60
Abou-El-Sherbini, K.S.; Pape, C.; Rienitz, O.; Schiel, D.; Stosch, R.; Weidler, P. G.; Höll, W. H.: Stabilization of n-amionopropyl silica gel against hydrolysis by blocking silanol groups with TiO2 or ZrO2. Journal of Sol-Gel Science and Technology 53 (2010) 587-597
Schiel, D.; Rienitz, O.: Einheitliche Analysen für sauberes Trinkwasser in Europa. GIT Labor-Fachzeitschrift, Nr. 54, 2/2010, 86
Rienitz, O.; Schiel, D.; Güttler, B.; Koch, M.; Borchers, U.: A convenient and economic approach to achieve SI-traceable reference values to be used in interlaboratory comparisons concerned with water analysis. CITAC News, LNE, February 2010
Mana, Giovanni; Rienitz, Olaf; Pramann, Axel: Measurement equations fort the determination of the Si molar mass by isotope dilution mass spectrometry. Metrologia 47 (2010) 460-463
Arsene, C.; Henrion, A.; Diekmann, N.; Manolopoulou, J.; Bidlingmaier, M.: Quantification of growth hormone in serum by isotope dilution mass spectrometry. Analytical Biochemistry, Elsevier, Vol. 401 (2010), Issue 2, pp. 228-235
Kaiser, P.; Akerboom, Th.; Ohlendorf, R.; Reinauer, H.: Liquid chromatography isotope dilution mass spectrometry as a new basis for the reference measurement procedure for Hemoglobin A1c determination. Clinical Chemistry (2010) 56:750-754
Feistel, R.; Weinreben, S.; Wolf, H.; Seitz, S.; Spitzer, P.; Adel, B.; Nausch, G.; Schneider, B.; Wright, D.G.: Density and Absolute Salinity of the Baltic Sea 2006-2009. Ocean Science (OS), 6, 3-24, 2010
Seitz, St.; Jensen, H.D.; Manzin, A.; Spitzer, P.; Jakobsen, P.T.: Traceability of electrolytic conductivity measurments to the International System of units in the sub mS/m region and review of models of electrolytic conductivity cells. Electrochimica Acta: 55 (2010), 22, 6323 - 6331
Spitzer, P.; Werner, B.; Jehnert, D.; Adel, B.: Zuverlässige Kalibrierung von pH-Messeinrichtungen. Traceable Calibration of pH Measurement Devices. tm-Technisches Messen 77 (2010) Heft 3, S. 156-161
Spitzer, P.; Pratt, K.: The history and development of a rigorous metrological basis for pH measurements. Journal of Solid State Electrochemistry (JSEL) (2010)
McDougall, T.J.; Feistel, R.; Wright, D.G.; Pawlowicz, R.; Millero, F.J.; Jackett, D.R.; King, B.A.; Marion, G.A.; Seitz, S.; Spitzer, P.; Chen, C.-T.A.: IOC, SCOR and IAPSO, 2010: The international thermodynamic equation of seawater ‐ 2010: Calculation and use of thermodynamic properties. Intergovernmental Oceanographic Commission, Manuals and Guides No. 56, UNESCO (English), 182 pp [Buch]
2009
Welsch, A.-M.; Maier, B. J.; Engel, J. M.; Mihailova, B.; Angel, R. J.; Paulmann, C.; Gospodinov, M.; Friedrich, A.; Stosch, R.; Güttler, B.; Petrova, D.; Bismayer1, U.: Effect of Ba-incorporation on pressure-induced structural changes in the relaxor ferroelectric PbSc0.5Ta0.5O3. Physical Review B 80 (2009) 104118-1 – 104118-7
Zakel, S.; Yaghobian, F.; Güttler, B.; Stosch, R.: Surface-Enhanced Raman Scattering (SERS). 248. PTB-Seminar Nanopartikel-Charakterisierung, PTB Braunschweig [poster], PTB-Bericht: PTB-CP-4, Juli 2009
Seitz, St.; Spitzer, P.; Brown, R.J.C.: CCQM-P111 study on traceable determination of practical salinity and mass fraction of major seawater components. Accreditation and Quality Assurance, 2009
Spitzer, P.; Fisicaro, P.; Seitz, St.; Champion, R.: pH and electrolytic conductivity as parameters to characterize bioethanol. Beitrag zum Sonderheft der Zeitschrifft AQUAL (Accreditation and Quality Assurance) zum Thema „Biofuel Metrology“, 2009
Seitz, St.; Spitzer, P.; Jakobsen, P.T.; Jensen, Hans D.: Metrological traceability concept for electrolytic conductivity and pH. CHIMIA, 2009
Fiedemann, M.; Pierz, K.; Stosch, R.; Ahlers, F.-J.: Graphene on gallium arsenide: Engineering the visibility, Applied Physics Letters, 95 (2009)
Güttler, B.: Activities of the EURAMET Technical Committee for Metrology in Chemistry. CITAC News, February 2009
Welsch, Anna-Maria; Mihailova, B.; Gospodinov, M.; Stosch, R., Güttler, B.; Bismayer, U.: High pressure Raman spectroscopic study on the relaxor ferroelectric PbSc0.5Nb0.5O3. Journal of Physics: Condensed Matter 21 (2009) 235901 (6pp)
Güttler, Bernd; Fisicaro, P.; Goenag-Infante, H.; Gören, A.C.; Jensen, H.D.; Kübarsepp, T.; Leito, I.; Lorefice, S.; Magnusson, B.; Mariassy, M.; Wunderli, S.: Traceable measurements for biospecies and ion activity in clinical chemistry. Konferenzband International Congress of Metrology 2009, Paris, France, 22-25, Juni, 2009
Güttler, B.; Richter, W.: Traceability of Chemical Measurement Results. Metrology, CHIMIA 2009, 63, No. 10, 1-5, Schweizerische Chemische Gesellschaft
Maier, B.; Mihailova, B.; Paulmann, C.; Ihringer, J.; Gospodinov, M.; Stosch, R.; Güttler, B.; Bismayer, U.: Effect of local elastic strain on the structure of Pb-based relaxors: A comparative study of pure and Ba- and Bi-doped PbSc0.5Nb0.5O3. Physical Review B 79, 224108 (2009)
Wang, Xiaojie; Mihailova, Boriana; Klocke, Arndt; Fittschen, Ursula E.A.; Heidrich, Stefanie; Hill, Mathias; Stosch, Rainer; Güttler, Bernd; Broekaert, José A.C.; Bismayer, Ulrich: Side effects of a non-peroxide-based home bleaching agent on dental enamel. Journal of Biomedical Materials Research Part A, Volume 88A, Issue 1, Date: January 2009, pp. 195-204
Turchanin, A.; Beyer, A.; Nottbohm, C. T.; Zhang, X.; Stosch, R.; Sologubenko, A.; Mayer, J.; Hinze, P.; Weimann, T.; Gölzhäuser, A.: One Nanometer Thin Carbon Nanosheets with Tunable Conductivity and Stiffness. Advanced Materials 21 (2009) 1233-1237
Máriássy, Michal; Pratt, Kenneth W.; Spitzer, Petra: Major applications of electrochemical techniques at national metrology institutes. Metrologia 46 (2009), 199–213
2008
Swart, C.; Simon, J.: Analyseverfahren zur Bestimmung von Proben mit silikatischer Matrix. Ein Vergleich am Beispiel römischer Ziegel. SKYLLIS, Zeitschrift für Unterwasserarchäologie, 8. Jahrgang 2007/2008, Heft 1-2, S. 37-42
Rienitz, Olaf: Messunsicherheit für Standardadditionsverfahren kombiniert mit innerem Standard und gravimetrischer Präparation am Beispiel der Rh-Bestimmung in Automobilkatalysatoren. Tagungsbericht 4. VDI Fachtagung „Messunsicherheit praxisgerecht bestimmen“, VDI Wissensforum, 2008
Sattouf, Mamdoh; Kratz, Sylvia; Diemer, Katrin; Fleckstein, Jürgen; Rienitz, O., Schiel, D.; Schnug, Ewald: Significance of uranium and strontium istotope ratios for retracing the fate of uranium during the processing of phosphate fertilizers from rock phosphates. In Buch: “Loads and Fate of Fertilizer-derived Uranium”, S 191-202, eds. L.J. De Kok & E. Schnug, Backhuys Publishers, Leiden, 2008
Seitz, S.; Spitzer, P.; Brown, Richard J.C.: Consistency of practical salinity measurements, traceable to primary conductivity standards: EUROMET project 918. Accreditation Quality Assurance 13:601-605 (2008)
Schiel, D.: Was leistet die Metrologie. Labor Praxis 32 (2008), S. 24-25
Mihailova, B.; Angel, R.J.; Welsch, A.-M.; Zhao, J.; Engel, J.; Paulmann, C.; Gospodinov, M.; Ahsbahs, H.; Stosch, R.; Güttler, B.; Bismayer, U.: Pressure-induced phase transition in PbSc0.5Ta0.5O3 as a model Pb-based perovksite-type relaxor ferroelectric. Physical Review Letters 101, No. 1, 017602 (2008)
Mihailova, B.; Maier, B.; Paulmann, C.; Malcherek, T.; Ihringer, J.; Gospodinov, M.; Stosch, R.; Güttler, B.; Bismayer, U.: High-temperature structural transformation in relaxor-ferroelectric PbSc0.5Ta0.5O3 and Pb0.78Ba0.22Sc0.5Ta0.5O3. Physical Review B, Vol. 77, 2008
Kleine-Ostmann, Thomas; Wilk, Rafal; Rutz, Frank; Koch, Martin; Niemann, Henning; Güttler, Bernd; Brandhorst, Kai; Grundenberg, Jörg: Probing noncovalent interactions in biomolecular crystals with terahertz spectroscopy. ChemPhysChem, 2008, 9, 544-547
Sattouf, Mamdoh; Diemer, Katrin; Kratz, Sylvia; Fleckenstein, Jürgen, Rienitz, Olaf; Schiel, Detlef; Schnug, Ewald: Isotopischer "Fingerabdruck" für Rohphosphate und Phosphor-Düngemittel. LaborPraxis, Journal für Labor, Analytik und Life Sciences, 2008, 32. Jahrgang, S. 26-28
Schiel, Detlef; Güttler, Bernd; Rienitz, Olaf; Matschat, Ralf; Koch, Michael; Borchers, Ulrich: Der Weg zu international vergleichbaren Messergebnissen. GCCh, Nachrichten aus der Chemie, 04/2008, S. 455-456
Burkitt, William I.; Pritchard, Caroline; Arsene, Cristian; Henrion, André; Bunk, David; O’Connor, Gavin: Toward Système International d’Unité-traceable protein quantification: From amino acids to proteins. Analytical Biochemistry, Volume 376, Issue 2 (2008), p.242-251
Lott,S.; Henrion,A.; Malz,F.; Kessler,A.; Güttler,B.; Aderjan,R.: Reference measurement procedure for Δ9-Tetrahydrocannabinol in serum.
Anal Bioanal Chem 391 (2008)1003
Arsene, C.G.; Ohlendorf, R.; Burkitt, W.; Pritchard, C.; Henrion, A.; O’Connor, G.; Bunk, D.M.; Güttler, B.: Protein Quantification by Isotope Dilution Mass Spectrometry of Proteolytic Fragments: Cleavage Rate and Accuracy.
Anal. Chem. 80, 4154–4160 (2008)
Spitzer, Petra; Giera, Janine; Fraga, Isabel C.; Tønnes Jakobsen, Pia; Jensen, Hans D.; Hyllested, Peter; Karpov, Oleg; Kutovoy, Viatcheslav; Nakamura, Susumu; Vospelova, Alena; Zvezdina, Valentina: Final report on CCQM-K9.2: Subsequent key comparison on pH determination of phosphate buffer by Harned cell measurements. 2008 Metrologia 45
2007
Rienitz, O.; Schiel, D.; Güttler, B.; Koch, M.; Borchers, U.: A convenient and economic approach to achieve SI-traceable reference values to be used in drinking-water interlaboratory comparisons. Accreditation and Quality Assurance 12, 2007, 615-622
Lott, S.; Protzek, C.; Aderjan, R.: Feldstudie zur Validierung eines optimierten Doppelstreifentestes für Cannabinoide im Urin zur effizienteren Erfassung von Fällen des § 24a STVG. Field study for validating an optimized dual-test for cannabionoids in urine for a more efficient determination of cases regarding legislation (§ 24a StVG). BLUTALKOHOL, vol. 44 (2007), S. 345 – 359
Maksimov, I.; Ohata, M.; Hioki, A.; Chiba, K.; Spitzer, P.: Development of Primary pH Method for Carbonate Standard Buffer Solution. BERM 11 (11th International Symposium on Biological and Environmental Reference Materials), Epochal Tsukuba, Japan, 29.10.-02.11.2007 [poster P-13]
Schiel, D.; Labarraque, Guillaume; Matschat, Ralf; Quetel, Christoph: EUROMET-project for the development of a metrological dissemination system providing Europe-wide comparable measurement results in water analysis under the WFD. [poster] WFD Conference, Lille (FR) 12.-14.03.2007
Mihailova, B.; Gospodinov, M.; Güttler, B.; Stosch, R.; Bismayer, U.: Ferroic clustering and phonon anomalies in Pb-based perovksite-type relaxors. J. Phys.: Condens. Matter 19 (2007)
Mihailova, B.; Gospodinov, M.; Güttler, B.; Petrova, D.; Stosch, R.; Bismayer, U.: Ferroic nanoclusters in relaxors: the effect of oxygen vacancies. Journal of Physics: Condensed Matter 19 (2007)
Willer, Ulrike; Wilk, Rafal; Schippers, Wolfgang; Böttger, Stephan; Nodop, Dirk; Schossig, T.; Schade, Wolfgang; Mikulics, Martin; Koch, Martin; Walther, Martin; Niemann, H.; Gütter, B.: A novel THz source based on a two-color Nd:LSB microchip-laser and a LT-GaAsSb photo-mixer. Applied Physics B: Laser and Optics, 87, 13-16 (2007)
Mihailova, B.; Bastjan, M. Schulz, B., Rübhausen, M.; Gospodinov, M.; Stosch, R.; Güttler, B.; Malcherek, T.; Bilmayer, U.: Resonance Raman scattering of relaxors PbSc0.5Ta0.5O3 and PbSc0.5Nb0.5O3. Applied Physics Letters 90, 042907 (2007)
Wang, X.; Klocke, A.; Mihailova, B.; Stosch, R.; Güttler, B.; Bismayer, U.: Effect of Bleaching on Dental Hard Tissues: a Raman and IR-Spectroscopic Study. Key Engineering Materials Vols. 330-332 (2007) pp. 1405-1408
Padilla-Viquez, Gerardo J.; Koelliker-Delgado, Jorge; Werhahn, O.; Jousten, Karl; Schiel, D.: Traceable CO2-R(12) line intensity for laser-spectroscopy-based gas analysis near 2 µm. IEEE Transactions on Instrumentation and Measurement Journal, Vol. 56, No. 2, April 2007, p. 529-533
Valkiers, S.; Varlam, M.; Ruβe, K.; Berglund, M.; Taylor, P.; Wang, J.; Milton, M.; De Bièvre, P.: Quantification of the degree-of-isotopic-equilibrium of carbon and oxygen isotopes in mixtures of CO2 gases. International Journal of Mass Spectrometry, Volume 263, Issues 2-3, 1 June 2007, Pages 195-203
Valkiers, S.; Varlam, M.; Ruße, K.; Berglund, M.; Taylor, P.; Wang, J.; Milton, M.J.T.; De Bièvre, P.: Preparation of Synthetic Isotope Mixtures for the calibration of carbon and oxygen isotope ratio measurements (in carbon dioxide) to the SI. International Journal of Mass Spectrometry, Volume 264, Issue 1, 15 June 2007, Pages 10-21
Schiel, D.; Labarraque, G.; Matschat, R.; Quetel, Ch.: EUROMET-project for the development of a metrological dissemination system providing Europe-wide comparable measurement results in water analysis under the WFD. WFD Conference, Lille (France), 12-14, March, 2007
Klocke, A.; Mihailova, B.; Zhang, S.; Casharova, B.; Stosch, R.; Güttler, B.; Henriot, P.; Ritschel, B.; Bismayer, U.: CO2 laser-induced zonation in dental enamel: a Raman and IR micro-spectroscopic study. Journal of Biomedical Materials Research: Part B: 81 (2007), 2, 499 - 507
Song Xiaoping, Petra Spitzer and Uwe Sudmeier: Novel method for bulk resistance evaluation in con-ductivity measurement for high-purity water, Accred. Qual. Assur. (2007) on-line first:DOI:10.1007/s00769-007-0258-5
Srecko F. Oman, M. Filomena Camões, Kipton J. Powell, Raj Rajagopalan, and Petra Spitzer: Guidelines for potentiometric measurements in suspensions Part B. Guidelines for practical pH measurements in soil suspensions (IUPAC Recommendations 2006) Pure and Applied Chemistry (2007), Vol. 79, Issue 1
Srecko F. Oman, M. Filomena Camões, Kipton J. Powell, Raj Rajagopalan, and Petra Spit-zer: Guidelines for potentiometric measurements in suspensions Part A. The suspension effect (IUPAC Technical Report) Pure and Applied Chemistry (2007) Vol. 79, Issue 1
2006
Marinova, V.; Mihailova, B.; Malcherek, T.; Paulmann, C.; Lengyel, K.; Kovacs, L.; Veleva, M.; Gospodinov, M.; Güttler, B.; Stosch, R.; Bismayer, U.: Structural, optical and dielectric properties of relaxor-ferroelectric Pb0.78Ba0.22Sc0.5Ta0.5O3. Journal of Physics: Condensed Matter 18 (2006) L385-L393, doi:10.1088/0953-8984/18/31/L01
Rienitz, O.; Röhker, K.; Schiel, D.; Han, J.; Oeter, D.: New equation for the evaluation of standard addition experiments applied to ion chromatography. Microchimica Acta 154, 21-25 (2006), ISSN 0026-3672 (print), ISSN 1436-5073 (online)
Werhahn, O.; Koelliker Delgado, J.; Niehoff, A.; Schiel, D.; Padilla Viques, G.J.; Jousten, K.: QUANSYS-Teilvorhaben Metrologische Grundlagen für Quantenkaskadenlaser-Gasmesssysteme: Verbundprojekt: Einmodige Quantenkaskadenlaser für Anwendungen in der Medizin-, Umwelt- und Produktionstechnik; Abschlussbericht., Laufzeit des Teilvorhabens: 01.07.2002-30.06.2005, BMBF-FKZ: 13N8123, Verbund-Nr. 01020466, PTB, 40 Seiten, März 2006
Matschat, R.; Kipphardt, H.; Rienitz, O.; Schiel, D.; Gernand, W.; Oeter, D.: Traceability system for elemental analysis. Accreditaion and Quality Assurance, Vol. 10, Heft 11, 2006 (ISSN 0949-1775), S. 633-639
Koelliker Delgado, J.; Werhahn, O.; Schiel, D.: IR-Spectrometric amount of CO2 fraction de-termination in gas analysis applications. 5. Konferenz über Optische Analysenmesstechnik in Industrie und Umwelt (OPTAM) 2006, 26.-27.09.2006, Mannheim; Poster in: VDI-Berichte "Anwendungen und Trends in der Optischen Analysenmesstechnik" (2006), Nr. 1959, S. 303-313
Werhahn, O.; Ulbig, P.: Rückführbarkeit in der spektrometrischen Gasanalytik. PTB-Bericht PTB-CP-2, Januar 2007, zum 226. PTB-Seminar am 22.-23. November 2006
Koelliker Delgado, J.; Werhahn, O.; Schiel, D.: IR-Spectrometric amount of CO2 fraction de-termination in gas analysis applications. Konferenzband zur "OPTAM-Tagung 2006", 26.-27.09.2006, Mannheim, Veröffentlichung im VDI-Bericht 1959, 2006
Becker, P.; Schiel, D.; Pohl, H.-J.; Kalitievski, A.K.; Godisov, O.N.; Churbanov, M.F.; Devyatykh, G.G.; Gusev, A.V.; Bulanov, A.D.; Adamchik, S.A.; Gavva, V.A.; Kovalev, I.D.; Abrosimov, N.V.; Hallmann-Seiffert, B.; Riemann, H.; Valkiers, S.; Taylor, P.; De Bievre, P. ; Dianov, E.M.: Large-scale production of highly enriched 28Si for the precise determination of the Avogadro constant, Measurement Science and Technology 17 (2006), 1854-1860
Dissertation:
Koelliker Delgado, J.: Amount of Carbon Dioxide Fraction Determination by TDLAS: Evidences for a Potential Primary Method Directly Applied in Gas Analysis. TU-Braunschweig Dissertation, 2006 (URL: www.digibib.tu-bs.de)
Padilla-Viquez, G. [speaker]; Koelliker-Delgado, J.; Werhahn, O.; Jousten, K.; Schiel, D.: Traceable molecular line strengths for gas analysis applications. Poster in: Summary-Paper in: Book of Abstracts der "2006 Conference on Precision Electromagnetic Measurements", S. 692-693, ISBN 88-7992-228-9, Turin, Italien, 9-14 July 2006
G. Meinrath, M.F. Camões, P. Spitzer, H. Bühler, M. Máriássy, K. Pratt, C. Rivier: The IU-PAC Working Party "Comparable pH Measurement by Metrological Traceability", Traceability of pH in a metrological context, Combining and Reporting Analytical re-sults, Ed: M. Belli, Dec.2006, RSC Publ.
Petra Spitzer, Key comparison CCQM-K19 on pH: final report, Metrologia 43 No 1A (Technical Supplement 2006) 08015
Spitzer, P.: Electrolytic Conductivity. Chapter 9-3, Springer Handbook of Materials Measurement Methods, Eds: Czichos, H.; Saito, T.; Smith, L. (2006)
2005
Arsene, C.; Lancrajan, I.; Burkitt, W.; Pang, S.; O’Connor, G.; Bunk, D.; Henrion, A.: Prerequisits to Accuracy in Absolute Protein Quantification by Mass Spectrometry. Molecular & Cellular Proteomics 4 (8), 2005, 315
Mihailova, B.; Gospodinov, M.M.; Güttler, B.; Yen, F.; Litvinchuk, A.P.; Iliev M.N.: Temperature-Dependent Raman Spectra of HoMn205 and TbMn205. Physical Review B 71, 172301 (2005)
Mihailova, B.; Bismayer, U.; Güttler, B.; Gospodinov, M.M.; Boris, A.; Bernhard, C.; Aroyo, M.: Nanoscale phase transformations in relaxor-ferroelectriclead scandium tantalate and lead scandium niobate. Z. Kristallographie, 220 (2005), S. 740-747
Güttler, B.; Richter, W.: Ein metrologisches Rückführungssystem für die chemische Analytik in Deutschland. PTB-Mitteilungen, Heft 4, Dezember 2005
Werhahn, O.; Koelliker Delgado, J.; Schiel, D.: Kalibrationsfreie Bestimmung von Stoffmengenanteilen - Potenziale für Quantenkaskadenlaser in der Gasanalytik. Technisches Messen, Sonderheft zu den QUANKAS/QUANSYS-Verbünden, (2005),Vol. 72, Nr. 6, S. 396-405
Sennikov, P.G.; Kotereva, T.V.; Kurganov, A.G.; Andreev, B.A.; Niemann, H.; Schiel, D.; Emtsev, V.V.; Pohl, H.-J.: Spectroscopic parameters of LVM absorption bands of carbon and oxygen impurities in isotopic enriched silicon 28Si, 29Si and 30Si. Physik und Technik der Halbleiter 39 (2005), S. 320-326
Stosch, R.; Henrion, A.; Schiel, D.; Güttler, B: Surface-Enhanced Raman Scattering Based Approach for Quantitative Determination of Creatinine in Human Serum. Analytical Chemistry 77 (2005) 7386-7392.
Rienitz, O.; Jährling, R.; Schiel, D.; Matschat, R.; Kipphardt, H.; Gernand, W.; Oeter, D.: Rückführung in der Elementanalytik. PTB-Mitteilungen, Heft 4, Dezember 2005
Stosch, R.; Henrion, A.; Schiel, D.; Güttler, B.: Oberflächenverstärkte Ramanspektroskopie und Isotopenverdünnung - ein potentiell primäres Messverfahren für die Metrologie in der Chemie. PTB-Mitteilungen, Heft 4, Dezember 2005
Werhahn, O.: Laserspektrometrie für die Gasanalytik. PTB-Mitteilungen, Heft 4, Dezember 2005
Henrion, A.: Isotopenverdünnung in der Proteinanalytik. PTB-Mitteilungen, Heft 4, Dezember 2005
Schädel, S.: Analytische Bestimmung von Steroidhormonen mittels IDMS. PTB-Mitteilungen, Heft 4, Dezember 2005
Haas, U.; Giera, Janine; Sudmeier, Uwe; Eberhardt, Ralf; Spitzer, Petra: Ionenselektive Elektroden - Möglichkeiten und Grenzen einer Rückführung. PTB-Mitteilungen, Heft 4, Dezember 2005
Petra Spitzer, Bruno Rossi, Yves Gaignet, Stéphane Mabic and Uwe Sudmeier: New approach to calibrating conductivity meters in the low conductivity range, Accred. Qual. Assur. (2005) 10: 78-81
Petra Spitzer, Traceable measurements of pH, p. 206-211, Traceability in Chemical Measurement, Springer Berlin Heidelberg (2005)
Richter, W.; Güttler, B.: A national traceability system for chemical measurements. Beitrag in Buch: Traceability in Chemical Measurement, Springer Berlin/Heidelberg, 2005, pp. 141-146
Spitzer, P.; Sudmeier, U.; Eberhardt, R.; Haas, U.; Giera, J.: Zuverlässige Messung der Leitfähigkeit von Reinstwasser. PTB-Mitteilungen, Heft 4, Dezember 2005
Spitzer, P.; Charlet, Ph.; Eberhardt, R.; Karpov, O.V.; Philippe, R.; Rivier, C.; Maximov, I.; Sudmeier, U.: Final Report of EUROMET Project 696: pH determination of a phthalate buffer. Metrologia 42 (2005), Tech. Suppl., 08001 (http://www.bipm.org/utils/common/pdf/ final_reports/QM/K17/EUROMET.QM-K17.pdf)
2004
Röhker, K.; Rienitz, O.; Schiel, D.: Ion chromatographic precision measurement procedure for electrolytes in human serum: validation with the aid of primary measurement procedures. Accred. Qual. Assur (2004) 9:671-677
2002
Buck, R.P.; Rondinini, S.; Baucke, F.G.K.; Camoes, M.F.; Covington, A.K.; Milton, M.J.T.; Mussini, T.; Naumann, R.; Pratt, K.W.; Spitzer, P.; Wilson, G.S.: The Measurement of pH-Definition, Standards and Procedures. Pure and Appl Chem (2002) 74:2169.2200

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